X-ray Photoelectron Spectroscopy Axis Supra (KRATOS-XPS)

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Guarantor: Josef Polčák, Ph.D.
Instrument status: Some Issues Some Issues, 25.3.2024 13:55, XPS - there is about 3 times smaller signal than usually which is probably by new channel plate detector which Kratos support is going to change after supplying another new one. Sometimes it happened, that X-ray source HV trip down. I small modiffication was did and it will be tested also during users measurement. Zn2p peak was observed on standard samples inside SAC. It is not clear if it is just on standard samples or inside vacuum chamber. Further investigation will be performed and will be discussed with service support.
Equipment placement: CEITEC Nano - C1.38
Research group: CF: CEITEC Nano


Description:

AXIS SupraTM is an X-ray photoelectron spectrometer (XPS) with unrivalled automation and ease of use for materials surface characterisation. The patented AXIS technology ensures high electron collection efficiency in spectroscopy mode and low aberrations at high magnifications in parallel imaging mode.


Publications:

  • KEPIČ, P.; LIŠKA, P.; IDESOVÁ, B.; CAHA, O.; LIGMAJER, F.; ŠIKOLA, T., 2024: Pulsed laser deposition of Sb2S3 films for phase-change tunable nanophotonics. NEW JOURNAL OF PHYSICS 26(1), p. 1 - 8, doi: 10.1088/1367-2630/ad1696; FULL TEXT
    (ICON-SPM, KRATOS-XPS, LYRA, ALD, WITEC-RAMAN, RIGAKU9, WOOLLAM-VIS)
  • Nouseen, S.; Ghosh, K.; Pumera, M., 2024: Hydrofluoric acid-free etched MAX on 3D-printed nanocarbon electrode for photoelectrochemical hydrogen production. APPLIED MATERIALS TODAY 36, doi: 10.1016/j.apmt.2023.101995; FULL TEXT
    (RIGAKU3, VERIOS, LYRA, KRATOS-XPS, JASCO)
  • Bawab, B.; Thalluri, S. M.; Kolíbalová, E.; Zazpe, R.; Jelinek, L.; Rodriguez-Pereira, J.; Macak, J. M., 2024: Synergistic effect of Pd single atoms and nanoparticles deposited on carbon supports by ALD boosts alkaline hydrogen evolution reaction. CHEMICAL ENGINEERING JOURNAL 482, doi: 10.1016/j.cej.2024.148959; FULL TEXT
    (ALD, VERIOS, TITAN, KRATOS-XPS, RIGAKU3)
  • RONOH, K.; NOVOTNÝ, J.; MRŇA, L.; KNÁPEK, A.; SOBOLA, D., 2024: Analysis of processing efficiency, surface, and bulk chemistry, and nanomechanical properties of the Monel® alloy 400 after ultrashort pulsed laser ablation. MATERIALS RESEARCH EXPRESS 11(1), doi: 10.1088/2053-1591/ad184b; FULL TEXT
    (DEKTAK, MIRA-STAN, KRATOS-XPS, NANOINDENTER)
  • TKACHENKO, S.; BEDNAŘÍKOVÁ, V.; KSENZOVA, O.; REMEŠOVÁ, M.; SLÁMEČKA, K.; CIHLÁŘ, J.; BALÁŽ, M.; DEÁK, A.; ČELKO, L., 2023: Microstructure and reduction behavior of Mo powders doped with La2O3 and ZrO2 oxides using the spray drying method. JOURNAL OF ALLOYS AND COMPOUNDS 264, doi: 10.1016/j.jallcom.2023.171307; FULL TEXT
    (RIGAKU3, LYRA, KRATOS-XPS, LEICACOAT-NANO)

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